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Preparation and properties of low-temperature self-expanding foamed ceramics utilizing lepidolite mica ore and ceramic tile polishing waste
Case Studies in Thermal Engineering ( IF 6.8 ) Pub Date : 2024-04-27 , DOI: 10.1016/j.csite.2024.104455
Yali Hu , Cai Wu , Yani Lu , Jiafeng Li , Daopei Zhu

Foamed ceramics were prepared at temperatures of 1175 °C, 1200 °C, 1225 °C, 1250 °C, and 1275 °C using lepidolite mica ore, ceramic tile polishing waste, and fly ash as raw materials, with borax as a fluxing agent. The main source of the foaming material was determined as , followed by anorthite and iron oxide, based on the X-ray diffraction (XRD) patterns of the raw materials and the thermal analysis (TG-DTA) results of the raw materials and . The effects of the raw material ratio and borax content on the samples' phase composition, compressive strength, microstructure, thermal insulation, and corrosion resistance were systematically studied. The results show that the pore structure of the foamed ceramics sintered at 1225 °C with 25 wt% lithium mica ore, 50 wt% ceramic tile polishing waste and 25 wt% fly ash were uniform. However, based on the above ingredients, 18 wt% borax was added to reduce the firing temperature by 300 °C. After firing at 925 °C and holding for 30 min, the samples' average pore size, bulk density, compressive strength, and porosity were 0.58 mm, 0.66 g/cm, 10.256 MPa, and 83.1 wt%, respectively. It exhibits good thermal insulation and corrosion resistance, and its performance meets the requirements for building insulation materials, making it an energy-saving and environmentally friendly building material.

中文翻译:

利用锂云母矿和瓷砖抛光废料制备低温自膨胀泡沫陶瓷及其性能

以锂云母矿、瓷砖抛光废料、粉煤灰为原料,硼砂为助熔剂,在1175℃、1200℃、1225℃、1250℃、1275℃温度下制备泡沫陶瓷。 。根据原料的X射线衍射(XRD)图谱和原料的热分析(TG-DTA)结果确定发泡材料的主要来源为 ,其次是钙长石和氧化铁。系统研究了原料配比和硼砂含量对样品的物相组成、抗压强度、显微组织、隔热性能和耐腐蚀性的影响。结果表明,添加25 wt%锂云母矿、50 wt%瓷砖抛光废料和25 wt%粉煤灰在1225 ℃烧结的泡沫陶瓷的孔结构均匀。但在上述成分的基础上,添加了18wt%的硼砂,使烧成温度降低了300℃。在925℃下烧成并保温30分钟后,样品的平均孔径、堆积密度、抗压强度和孔隙率分别为0.58mm、0.66g/cm、10.256MPa和83.1wt%。具有良好的保温、耐腐蚀性能,其性能满足建筑保温材料的要求,是一种节能环保的建筑材料。
更新日期:2024-04-27
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